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Beilstein J. Org. Chem. 2010, 6, No. 27, doi:10.3762/bjoc.6.27
Graphical Abstract
Figure 1: Valsartan.
Scheme 1: Retrosynthetic analysis of 8.
Scheme 2: (a) Et3N, CH2Cl2, 0 °C, 95%; (b) NaH, THF, 70%; (c) n-BuLi, 25 °C, THF, anhyd ZnCl2, −20 °C, Q-phos...
Beilstein J. Org. Chem. 2010, 6, No. 25, doi:10.3762/bjoc.6.25
Figure 1: The angiotensin II receptor antagonist Telmisartan.
Scheme 1: First literature synthesis of Telmisartan (a) nPrCOCl, C6H5Cl, 100 °C (b) HNO3/H2SO4, 0 °C (c) Pd/C...
Scheme 2: (a) Pd(PPh3)4, aq Na2CO3, THF, 12.0 h, 90%.
Scheme 3: (a) p-TsOH, toluene, 110 °C, 12 h, (b) Pd/C, 7 bar H2, MeOH, 60 °C, 24 h, 100% (c) AcOH, 120 °C, 2 ...
Beilstein J. Org. Chem. 2009, 5, No. 80, doi:10.3762/bjoc.5.80
Figure 1: Aryl-1,2,3,4-tetrahydroisoquinolines.
Scheme 1: Retrosynthetic analysis of 5.
Scheme 2: (a) 1,2-Dimethoxybenzene, TFA, reflux, 3 h, 90%; (b) DIBAL-H, CH2Cl2, −78 °C, 3 h, 65%; (c) (i) NaN3...